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doi: 10.1111/ppa.12893 49 Mndez-LpezE.DonaireL.GoslvezB.Daz-VivancosP.Snchez-PinaM
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The derivatization protocol for the quantification of TMA was an adaptation of the protocol described by Samples for TMAO levels quantification were prepared as follows: an amount of 25 L of each sample was collected, and 3 L of D9-TMAO (5 M concentration) and 122 L of a cold acetonitrile:methanol mixture (50:50, v/v) were added for protein precipitation
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